CuK? radiation ; ? = 1,5406 Å à 44 KV et 30 mA) avec un générateur de type PW 1830, Les diffractogrammes sont mesurés pour un angle 2? variant entre 10° et 90°. Les images de microscopie électronique à balayage (MEB) ont été obtenues sur un ,
Japon) opérationnel jusqu'à 25 KV Tous les échantillons sont métallisés avec une fine couche de Au/Pd avant l'observation pour s'affranchir des phénomènes de "charge" des matériaux ,
ATG) étudiant la conversion du polymère en céramique ont été effectuées sur une thermobalance de type TGA, Setaram TGA 92, pp.16-18 ,
La vitesse de chauffage est fixée à 1°C ,
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